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bThese three complexes have typical spectra of high spin five coordinate iron(II) porphyrin complexes. However, at liquid nitrogen temperature, they all form some low-spin six-coordinate [Fe(PPIX)L2] complex (see Ref. [63])
eThis spectrum gave evidence for 45 (2)% of this low-spin complex and 23 (3)% of a five coordinate high spin complex believed to be [Fe(PPIX)(tButNH2)] and 32 (2)% of the unreacted (none ligated to tButNH2) starting [Fe(PPIX)]
J.S thanks ICI for support for part of this work. We also thank the glass blower at Essex University for assembling the glass cryostat and the glass to metal joint (for the silica sample cell) used for the low-temperature electronic spectra recorded herein.
Investigators say they found some of the images on a work laptop computer Stuart Forrest was carrying out of his San Mateo home on Dec. 20, hours after he was first interviewed at his office by San Jose police detectives and just before the search, according to a U.S. Postal Inspection Service report obtained by this newspaper.
The report provides the first detailed account of the secretive federal investigation, which resulted in state prosecutors charging Forrest with two felony counts of child pornography possession in February. He retired after 35 years working for the county, 11 days after the search. He is out on bail ahead of his July 15 trial date in San Mateo County Superior Court and has vowed to fight the charges.
Leanos said his client had the images, found on a work laptop and a thumb drive at his office, as part of an effort to teach probation officers to identify child porn. Law enforcement agents are protected from prosecution if they have child porn for training or an investigation.
The charges against Forrest stunned many in the county establishment. He was a serious, quiet bureaucrat who, since San Mateo County Superior Court judges appointed him in 2009, steered the probation department and its $75 million budget without much controversy.
At about 3:45 p.m., federal agents were waiting for a search warrant when they spotted Forrest carrying a bag out of the San Mateo house. They already searched the Tracy home that afternoon, without apparently finding any child porn.
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